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Visible light induced cooperative carbonylation and (hetero)aryl migration: synthesis of multi-carbonyl compounds

Hefei Yang, Yuanrui Wang, Le‐Cheng Wang, Xiao‐Feng Wu

2024Chemical Science20 citationsDOIOpen Access PDF

Abstract

Carbonylative transformation represents one of the most straightforward procedures for the synthesis of carbonyl-containing compounds. However, the carbonylative procedure toward 1,4-diketones is still limited which are key moieties with potent applications in various areas. Herein, we report a new strategy for the synthesis of multi-carbonyl compounds containing a 1,4-diketone skeleton through remote heteroaryl migration of traditionally restricted 1,3-migratory substrates utilizing carbon monoxide (CO) as the C1 synthon and diazonium compounds as the starting material.

Topics & Concepts

CarbonylationArylCombinatorial chemistryChemistryVisible spectrumPhotochemistryCatalysisOrganic chemistryMaterials scienceCarbon monoxideAlkylOptoelectronicsCatalytic C–H Functionalization MethodsRadical Photochemical ReactionsCyclopropane Reaction Mechanisms