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K <sub>3</sub> SbS <sub>4</sub> as a Potassium Superionic Conductor with Low Activation Energy for K–S Batteries

Jieren Shao, Jingfeng Zheng, Lei Qin, Songwei Zhang, Yang Ren, Yiying Wu

2022Angewandte Chemie12 citationsDOIOpen Access PDF

Abstract

Abstract Solid‐state K‐ion conducting electrolytes are key elements to address the current problems in K secondary batteries. Here, we report a sulfide‐based K‐ion conductor K 3 SbS 4 with a low‐activation energy of 0.27 eV. W‐doped K 3− x Sb 1− x W x S 4 ( x =0.04, 0.06, 0.08, 0.10 and 0.12) compounds were also explored for increasing vacancy concentrations and improving ionic conductivity. Among them, K 2.92 Sb 0.92 W 0.08 S 4 exhibits the highest conductivity of 1.4×10 −4 S cm −1 at 40 °C, which is among the best reported potassium‐ion conductors at ambient temperature. In addition, K 2.92 Sb 0.92 W 0.08 S 4 is electrochemically stable with long‐chained potassium polysulfide of K 2 S x . A room‐temperature solid potassium–sulfur (K−S) battery system has therefore been successfully demonstrated, which is the first K−S battery prototype using non‐commercial inorganic‐based electrolyte to block the polysulfide shuttle.

Topics & Concepts

PolysulfideElectrolytePotassiumFast ion conductorConductivityIonic conductivityActivation energyChemistryBattery (electricity)SulfideIonInorganic chemistryAnalytical Chemistry (journal)Materials sciencePhysical chemistryElectrodeThermodynamicsChromatographyPower (physics)Organic chemistryPhysicsAdvanced Battery Materials and TechnologiesThermal Expansion and Ionic ConductivitySolid-state spectroscopy and crystallography
K <sub>3</sub> SbS <sub>4</sub> as a Potassium Superionic Conductor with Low Activation Energy for K–S Batteries | Litcius