Elaboration of Functionalized Iron Oxide Nanoparticles by Microwave-Assisted Co-Precipitation: A New One-Step Method in Water
Thomas Girardet, Amel Cherraj, Pierre Venturini, Hervé Martinez, Jean‐Charles Dupin, Franck Cleymand, Solenne Fleutot
Abstract
Iron oxide nanoparticles are extensively utilized in various fields, particularly in biomedical applications. For such uses, nanoparticles must meet specific criteria, including precise size, morphology, physico-chemical properties, stability, and biocompatibility. Microwave-assisted co-precipitation offers an efficient method for producing water-soluble nanoparticles. Functionalization with citrate during synthesis is crucial for achieving a stable colloidal solution. This study aims to compare the effectiveness of conventional co-precipitation with microwave-assisted co-precipitation. The synthesized nanoparticles were characterized using TEM, DLS, FTIR, XRD, and magnetic measurements. The findings indicate that the in situ citrate functionalization during synthesis results in stable, non-aggregated nanoparticles.