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Discovery of High-Affinity Amyloid Ligands Using a Ligand-Based Virtual Screening Pipeline

Timothy S. Chisholm, Mark Mackey, Christopher A. Hunter

2023Journal of the American Chemical Society41 citationsDOIOpen Access PDF

Abstract

; a machine learning model based on simple chemical descriptors; and machine learning models that use field points as a 3D description of shape and surface properties in the Forge software. The three-step pipeline was used to virtually screen 698 million compounds from the ZINC15 database. From the top 100 compounds with the highest predicted affinities, 46 compounds were experimentally investigated by using a thioflavin T fluorescence displacement assay. Five new Aβ(1-42) ligands with dissociation constants in the range 20-600 nM and novel structures were identified, demonstrating the power of this ligand-based approach for discovering new structurally unique, high-affinity amyloid ligands. The experimental hit rate using this virtual screening approach was 10.9%.

Topics & Concepts

ChemistryVirtual screeningLigand (biochemistry)Pipeline (software)Amyloid (mycology)Computational biologyCombinatorial chemistryDrug discoveryBiochemistryReceptorProgramming languageBiologyComputer scienceInorganic chemistryComputational Drug Discovery MethodsBioinformatics and Genomic NetworksProtein Structure and Dynamics
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