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Experimental and theoretical approaches on structural, spectroscopic (FT‐IR and UV‐Vis), nonlinear optical, and molecular docking analyses for Zn (II) and Cu (II) complexes of 6‐chloropyridine‐2‐carboxylic acid

Necmi Dege, Ömer Tamer, Merve Şimşek, Davut Avcı, M. Yaman, Adi̇l Başoğlu, Yusuf Atalay

2022Applied Organometallic Chemistry71 citationsDOI

Abstract

Abstract Novel transition metal‐based complexes that may be of value as biological agents and/or nonlinear optical materials, Zn (II) and Cu (II) transition metal complexes of 6‐chloropyridine‐2‐carboxylic acid (LH), were successfully synthesized. The chemical structure of each complex was characterized using X‐ray diffraction (XRD) method and FT‐IR spectroscopy. XRD and FT‐IR demonstrated that L ligand coordinate to central metal ions through the donor N and O atoms. By coordinating two H 2 O ligand to Zn (II) ion, a distorted octahedral complex geometry was constructed for 1 . As for 2 , a distorted trigonal bipyramidal coordination geometry was obtained by a H 2 O ligand coordination to Cu (II) ion. Theoretical studies using B3LYP/6‐311++G(d,p)‐LanL2DZ were performed to further validate the proposed structures. The molecular docking of 1 to SARS‐CoV‐2 main protease (PDB: 6LU7) gives a binding energy of −5.24 kcal/mol and inhibition constant of 144.6 μM, demonstrating that 1 is a more promising candidate to biologically active complexes than 2 . The first‐order hyperpolarizability (β) parameter for 1 and 2 was calculated as 0.88 × 10 −30 and 10.40 × 10 −30 esu, respectively. These β values also demonstrated that 2 exhibits more effective NLO character than 1 due to the electronic configuration and coordination geometry.

Topics & Concepts

ChemistryHyperpolarizabilityCrystallographyCoordination complexLigand (biochemistry)Trigonal bipyramidal molecular geometryOctahedral molecular geometryOctahedronMetal ions in aqueous solutionTransition metalMetalCoordination geometryDocking (animal)StereochemistryMoleculeCrystal structureHydrogen bondOrganic chemistryBiochemistryReceptorNursingCatalysisMedicinePolarizabilityNonlinear Optical Materials ResearchMetal complexes synthesis and propertiesCrystal structures of chemical compounds
Experimental and theoretical approaches on structural, spectroscopic (FT‐IR and UV‐Vis), nonlinear optical, and molecular docking analyses for Zn (II) and Cu (II) complexes of 6‐chloropyridine‐2‐carboxylic acid | Litcius