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Substrate-controlled C–H or C–C alkynylation of cyclopropanes: generation of aryl radical cations by direct light activation of hypervalent iodine reagents

Tin V. T. Nguyen, Matthew D. Wodrich, Jérôme Waser

2022Chemical Science28 citationsDOIOpen Access PDF

Abstract

C–C or C–H alkynylation of aryl cyclopropanes was realized by direct activation of EBX reagents with visible light. With ortho methyl groups on the benzene, C–H functionalization became favoured.

Topics & Concepts

Hypervalent moleculeArylIodineAlkynylationReagentChemistrySubstrate (aquarium)PhotochemistryCombinatorial chemistryMedicinal chemistryCatalysisOrganic chemistryAlkylOceanographyGeologyOxidative Organic Chemistry ReactionsCatalytic C–H Functionalization MethodsRadical Photochemical Reactions
Substrate-controlled C–H or C–C alkynylation of cyclopropanes: generation of aryl radical cations by direct light activation of hypervalent iodine reagents | Litcius