Litcius/Paper detail

DL‐EPR and AFM study of sensitization of a 17%Cr multiphase stainless steel

Sérgio Souto Maior Tavares, Marcelo T. G. de Sampaio, Gerónimo Pérez, Brígida Bastos de Almeida, Eduardo A. Ponzio

2022Materials and Corrosion13 citationsDOI

Abstract

Abstract The corrosion behavior of a 17Cr multiphase martensitic stainless steel quenched (1000°C, water cooling) and tempered at different temperatures was determined using the double‐loop electrochemical potentiokinetic reactivation (DL‐EPR) test. The specimen tempered at 550°C showed the highest degree of sensitization. For the specimen treated at 600°C, a healing process was observed, followed by a second sensitization at 625°C coincident with an increase in the austenite volume fraction. This phase was quantified using the magnetic method and an increase in this phase was observed with the tempering temperature. The DL‐EPR results were correlated with surface aspects obtained by atomic force microscopy.

Topics & Concepts

TemperingMaterials scienceMartensiteSensitizationElectron paramagnetic resonanceVolume fractionAusteniteAtomic force microscopyMetallurgyPhase (matter)Double loopAnalytical Chemistry (journal)Composite materialNuclear magnetic resonanceChemistryMicrostructureNanotechnologyChromatographyImmunologyProcess managementOrganic chemistryBusinessPhysicsBiologyHydrogen embrittlement and corrosion behaviors in metalsCorrosion Behavior and InhibitionWelding Techniques and Residual Stresses