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Strong Coupling and Slow Relaxation of the Magnetization for an Air-Stable [Co<sub>4</sub>] Square with Both Tetrazine Radicals and Azido Bridges

Zhilin Guo, Yi‐Fei Deng, Zoe Pikramenou, Kim R. Dunbar, Yuan‐Zhu Zhang

2021Inorganic Chemistry15 citationsDOI

Abstract

Introducing both tetrazine radical and azido bridges afforded two air-stable square complexes [MII4(bpztz•–)4(N3)4] (MII = Zn2+, 1; Co2+, 2; bpztz = 3,6-bis(3,5-dimethylpyrazolyl)-1,2,4,5-tetrazine), where the metal ions are cobridged by μ1,1-azido bridges and tetrazine radicals. Magnetic studies revealed strong antiferromagnetic metal–radical interaction with a coupling constant of −64.7 cm–1 in the 2J formalism in 2. Remarkably, 2 exhibits slow relaxation of magnetization with an effective barrier for spin reverse of 96 K at zero applied field.

Topics & Concepts

ChemistryTetrazineRadicalMagnetizationMetalCoupling constantAntiferromagnetismFormalism (music)CrystallographyMagnetic fieldComputational chemistryCondensed matter physicsOrganic chemistryPhysicsQuantum mechanicsArtMusicalVisual artsMagnetism in coordination complexesLanthanide and Transition Metal ComplexesOrganic and Molecular Conductors Research