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High-resolution calorimetry in pulsed magnetic fields

Shusaku Imajo, Chao Dong, Akira Matsuo, Koichi Kindo, Yoshimitsu Kohama

2021Review of Scientific Instruments20 citationsDOIOpen Access PDF

Abstract

We have developed a new calorimeter for measuring the thermodynamic properties in pulsed magnetic fields. Instrumental design is described along with the instrument construction details, including the sensitivity of a RuO2 thermometer. Operation of the calorimeter is demonstrated by measuring the heat capacity of three samples: pure germanium, CeCu2Ge2, and κ-(BEDT-TTF)2Cu[N(CN)2]Br, in pulsed fields up to 43.5 T. Obtaining field stability is key in measuring high-resolution heat capacity under pulsed fields. We also examine the performance of the calorimeter by employing two measurement techniques: the quasi-adiabatic and dual-slope techniques. We demonstrate that the calorimeter developed in this study is capable of performing high-resolution calorimetry in pulsed magnetic fields, which opens the door to new opportunities for high-field thermodynamic studies.

Topics & Concepts

Calorimeter (particle physics)CalorimetryMaterials scienceMagnetic fieldHeat capacityCalorimeter constantMeasuring instrumentTemperature measurementField (mathematics)Nuclear engineeringThermodynamicsSensitivity (control systems)Analytical Chemistry (journal)Heat-assisted magnetic recordingNuclear magnetic resonanceSpecific heatCalibrationRare-earth and actinide compoundsHigh-pressure geophysics and materialsChemical and Physical Properties of Materials
High-resolution calorimetry in pulsed magnetic fields | Litcius