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TEMPERATURE DEPENDENCES OF THE PECLET NUMBER IN SUBLIMATION PROCESSES OF SIMPLE SUBSTANCES

A. I. Kravchenko, A. I. Zhukov, O.A. Datsenko

202215 citationsDOIOpen Access PDF

Abstract

The results of calculating the Peclet number Ре = wr/(ρD) (where D is the diffusion coefficient; w is the evaporation rate of the substance; ρ is the density of the substance; r is the size factor) in sublimation processes of simple substances with high values of vapor pressure (≈ 1 mm Hg and above at the melting temperature): As, Gd, Tm, Lu, Cr, Yb, Sm, Mg, Ra, Ca, Sr, Ni, Co, Eu, Mn, Ba. It is shown that the nature of the temperature dependence Pe(T) is determined by the properties of the components of the sublimated system “base–impurity” (including the diffusion activation energy Q of impurity). For each substance for given Q and r, the dependence Pe(T) is monotonic. A decrease in the process temperature can improve the purification of a substance from one of several impurities, accompanied by deterioration in the purification from another impurity.

Topics & Concepts

Sublimation (psychology)ImpurityVapor pressureThermodynamicsActivation energyDiffusionChemistryPéclet numberAnalytical Chemistry (journal)EvaporationMaterials sciencePhysical chemistryChromatographyOrganic chemistryPhysicsPsychotherapistPsychologyChemical Thermodynamics and Molecular StructureMetallurgical Processes and ThermodynamicsThermal and Kinetic Analysis
TEMPERATURE DEPENDENCES OF THE PECLET NUMBER IN SUBLIMATION PROCESSES OF SIMPLE SUBSTANCES | Litcius