Litcius/Paper detail

Self‐Healing Metallo‐Supramolecular Hydrogel Based on Specific Ni<sup>2+</sup> Coordination Interactions of Poly(ethylene glycol) with Bistriazole Pyridine Ligands in the Main Chain

Xiaowen Xu, Valentin Victor Jerca, Richard Hoogenboom

2020Macromolecular Rapid Communications33 citationsDOIOpen Access PDF

Abstract

Abstract In this study, a supramolecular hydrogel formed by incorporating the 2,6‐bis(1,2,3‐triazol‐4‐yl)‐pyridine (btp) ligand in the backbone of a polymer prepared by copper(I)‐catalyzed alkyne‐azide cycloaddition (CuAAC) “click” polyaddition reaction of 2,6‐diethynylpyridine and diazido‐poly(ethylene glycol) is reported. The hydrogelation is selectively triggered by the addition of Ni 2+ ions to aqueous copolymer solutions. The gelation and rheological properties could be tuned by the change of metal to ligand ratio and polymer concentration. Interestingly, the hydrogel exhibits a fast (within 2 min) and excellent repeatable autonomic healing capacity without external stimuli. This self‐healing behavior may find potential applications for the repairing of metal coatings, in the future.

Topics & Concepts

Ethylene glycolSupramolecular chemistryPolymer chemistrySelf-healing hydrogelsAzideCycloadditionAqueous solutionPyridineAlkyneLigand (biochemistry)PolymerClick chemistryCopolymerMaterials scienceSupramolecular polymersEthyleneMetal ions in aqueous solutionMetalChemistryOrganic chemistryMoleculeCatalysisReceptorBiochemistryPolymer composites and self-healingDendrimers and Hyperbranched Polymers
Self‐Healing Metallo‐Supramolecular Hydrogel Based on Specific Ni<sup>2+</sup> Coordination Interactions of Poly(ethylene glycol) with Bistriazole Pyridine Ligands in the Main Chain | Litcius