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Microfluidic device integrating single‐cell extraction and electrical lysis for mass spectrometry detection of intracellular compounds

Tomáš Václavek, František Foret

2022Electrophoresis23 citationsDOI

Abstract

Analysis of cellular composition and metabolism at a single-cell resolution allows gaining more information about complex relationships of cells within tissues or whole living organisms by resolving the variance stemming from the cellular heterogeneity. Mass spectrometry (MS) is a perfect analytical tool satisfying the demanding requirements of detecting and identifying compounds present in such ultralow-volume samples of high chemical complexity. However, the method of sampling and sample ionization is crucial in obtaining relevant information. In this work, we present a microfluidic sampling platform that integrates single-cell extraction from MS-incompatible media with electrical cell lysis and nanoESI-MS analysis of human erythrocytes. Hemoglobin alpha and beta chains (300 amol/cell) were successfully identified in mass spectra of single-erythrocyte lysates.

Topics & Concepts

LysisMass spectrometryMicrofluidicsChromatographySample preparationSingle-cell analysisChemistrySampling (signal processing)Extraction (chemistry)IntracellularCellResolution (logic)Analytical Chemistry (journal)Biological systemComputational biologyComputer scienceNanotechnologyBiochemistryMaterials scienceBiologyArtificial intelligenceComputer visionFilter (signal processing)Mass Spectrometry Techniques and ApplicationsMicrofluidic and Capillary Electrophoresis ApplicationsAdvanced Proteomics Techniques and Applications
Microfluidic device integrating single‐cell extraction and electrical lysis for mass spectrometry detection of intracellular compounds | Litcius