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Simple Ether‐Directed Enantioselective C(<i>sp</i><sup>3</sup>)−H Borylation of Cyclopropanes Enabled by Iridium Catalysis

Tian Xie, Lili Chen, Zhenlu Shen, Senmiao Xu

2023Angewandte Chemie International Edition43 citationsDOIOpen Access PDF

Abstract

Abstract Reported here is an efficient and simple ether‐directed iridium‐catalyzed enantioselective C( sp 3 )−H borylation of cyclopropanes. Various functional groups were well‐tolerated, affording a vast array of chiral cyclopropanes with high enantioselectivities. We also demonstrated that the turnover numbers of the current reaction could be up to 335.

Topics & Concepts

BorylationEnantioselective synthesisIridiumChemistryCatalysisEtherCombinatorial chemistryOrganic chemistryMedicinal chemistryArylAlkylCatalytic C–H Functionalization MethodsCyclopropane Reaction MechanismsAsymmetric Hydrogenation and Catalysis
Simple Ether‐Directed Enantioselective C(<i>sp</i><sup>3</sup>)−H Borylation of Cyclopropanes Enabled by Iridium Catalysis | Litcius