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Methanol as a C1 Source for the Synthesis of 1,3‐Polyheterocyclic Systems

L. Molteni, Egle M. Beccalli, Laura Castoldi, Gianluigi Broggini, Camilla Loro

2023European Journal of Organic Chemistry10 citationsDOIOpen Access PDF

Abstract

Abstract A very attractive approach toward 1,3‐polyheterocyclic systems was provided exploiting the copper‐catalyzed reaction of aminoalcohols and diaminoalkanes, in oxidative conditions and in the presence of methanol. The synthetic pathway showed the involvement of methanol both as solvent and as a reagent, making the procedure particularly efficient and sustainable for the synthesis of five‐, six‐, and seven‐membered polyheterocyclic rings.

Topics & Concepts

ChemistryMethanolReagentCombinatorial chemistrySolventCatalysisOrganic chemistryAsymmetric Hydrogenation and CatalysisCyclopropane Reaction MechanismsCatalytic C–H Functionalization Methods
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