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Enhanced Hydride Donation Achieved Molybdenum Catalyzed Direct <i>N</i>-Alkylation of Anilines or Nitroarenes with Alcohols: From Computational Design to Experiment

Weikang Li, Ming Huang, Jiahao Liu, Yong‐Liang Huang, Xiao‐Bing Lan, Zongren Ye, Cunyuan Zhao, Yan Liu, Zhuofeng Ke

2021ACS Catalysis69 citationsDOI

Abstract

An example of homogeneous Mo-catalyzed direct N-alkylation of anilines or nitroarenes with alcohols is presented. The DFT aimed design suggested the easily accessible bis-NHC-Mo(0) complex features a strong hydride-donating ability, achieving effective N-alkylation of anilines or challenging nitroarenes with alcohols. The enhanced hydride-donating strategy should be useful in designing highly active systems for borrowing hydrogen transformations.

Topics & Concepts

AlkylationHydrideCatalysisChemistryMolybdenumHomogeneousCombinatorial chemistryHomogeneous catalysisHydrogenOrganic chemistryThermodynamicsPhysicsAsymmetric Hydrogenation and CatalysisNanomaterials for catalytic reactionsAmmonia Synthesis and Nitrogen Reduction
Enhanced Hydride Donation Achieved Molybdenum Catalyzed Direct <i>N</i>-Alkylation of Anilines or Nitroarenes with Alcohols: From Computational Design to Experiment | Litcius