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Effect of sintering temperature on the dielectric properties of 3D‐printed alumina (Al <sub>2</sub> O <sub>3</sub> ) in the W‐band

Kai‐Daniel Jenkel, Jesús Sánchez‐Pastor, Mohammad Mahdi Baloochian, Rolf Jakoby, Masoud Sakaki, Alejandro Jiménez‐Sáez, Niels Benson

2023Journal of the American Ceramic Society15 citationsDOIOpen Access PDF

Abstract

Abstract This contribution discusses the impact of sintering temperatures on dielectric properties of 3D‐printed alumina (Al 2 O 3 ) in the W‐band, by evaluating high quality factor (− Q ) resonators integrated in a 2D photonic crystal structure. By varying the sintering temperature of the lithography‐based ceramic manufactured (LCM) samples, the microstructure of the material can be defined, which has a direct impact on the dielectric permittivity and material losses. Using a highly accurate photonic crystal structure, with a dimensional variation below 2% from print to print, an accurate extraction and evaluation of the dielectric material properties could be achieved. The relative permittivity of the alumina was tuned from 4.4 at 1250°C to 9.2 at 1650°C, whereas the observed change in dielectric losses was moderate. The maximum in observed dielectric loss for samples sintered at the lowest evaluated temperature, only yields an average value of 30 × 10 −4 . This demonstrates the versatility of the LCM technology for mm‐ and sub‐mm‐wave applications and its possibilities for material tuneability.

Topics & Concepts

Materials scienceSinteringDielectricMicrostructureRelative permittivityCeramicPermittivityComposite materialPhotonic crystalDielectric lossOptoelectronicsMicrowave Dielectric Ceramics SynthesisFerroelectric and Piezoelectric MaterialsAdvanced ceramic materials synthesis
Effect of sintering temperature on the dielectric properties of 3D‐printed alumina (Al <sub>2</sub> O <sub>3</sub> ) in the W‐band | Litcius