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Enantioselective Syntheses of <i>C</i><sub>2</sub>-Symmetric Pyrazolones and Diones via One-Pot Organo-/Iodine Sequential Catalysis

Kai‐Xiang Feng, Cheng‐Ke Tang, Qiao‐Yu Shen, Ai‐Bao Xia, Lisha Huang, Zhan‐Yu Zhou, Xing Zhang, Xiaohua Du, Dan‐Qian Xu

2021Organic Letters12 citationsDOI

Abstract

The catalytic diastereo- and enantioselective syntheses of C2-symmetric axially chiral 1,4-dicarbonyl derivatives with 2,3-quaternary stereocenters were achieved by utilizing an organo-/iodine binary catalytic strategy. The reactions proceeded well under mild conditions without metals or strong bases.

Topics & Concepts

ChemistryEnantioselective synthesisStereocenterPyrazolonesCatalysisIodineOrganic chemistryCombinatorial chemistryMedicinal chemistryAxial and Atropisomeric Chirality SynthesisMolecular spectroscopy and chiralityAsymmetric Synthesis and Catalysis