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Synthesis of aromatic terminal allenes and aliphatic terminal alkynes from hydrazones using calcium carbide as an acetylene source

Lei Gao, Zheng Li

2020Organic Chemistry Frontiers55 citationsDOI

Abstract

A simple method for the selective synthesis of aromatic terminal allenes and aliphatic terminal alkynes from the reactions of calcium carbide with ketone and aldehyde <italic>p</italic>-tosylhydrazones using copper as a mediator is described.

Topics & Concepts

ChemistryCalcium carbideAcetyleneKetoneAldehydeTerminal (telecommunication)Organic chemistryHydrazoneCalciumCatalysisComputer scienceTelecommunicationsSynthesis and Characterization of PyrrolesCyclopropane Reaction MechanismsCatalytic Alkyne Reactions
Synthesis of aromatic terminal allenes and aliphatic terminal alkynes from hydrazones using calcium carbide as an acetylene source | Litcius