Litcius/Paper detail

Diradical Generation via Relayed Proton-Coupled Electron Transfer

Qianqian Shi, Zhipeng Pei, Jinshuai Song, Shijun Li, Donghui Wei, Michelle L. Coote, Yu Lan

2022Journal of the American Chemical Society80 citationsDOIOpen Access PDF

Abstract

Diradical generation followed by radical-radical cross-coupling is a powerful synthetic tool, but its detailed mechanism has yet to be established. Herein, we proposed and confirmed a new model named relayed proton-coupled electron transfer (relayed-PCET) for diradical generation, which could open a door for new radical-radical cross-coupling reactions. Quantum mechanics calculations were performed on a selected carbene-mediated diradical cross-coupling reaction model and a designed model, and the exact electronic structural changes during the radical processes have been observed for the first time.

Topics & Concepts

DiradicalChemistryElectron transferCoupling (piping)CarbeneProtonPhotochemistryElectronChemical physicsProton-coupled electron transferComputational chemistryRadicalAtomic physicsQuantum mechanicsCatalysisPhysicsExcited stateOrganic chemistrySinglet stateMechanical engineeringEngineeringRadical Photochemical ReactionsCatalytic C–H Functionalization MethodsCO2 Reduction Techniques and Catalysts