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Understanding dynamic voltammetry in a dissolving microdroplet

Ashutosh Rana, Christophe Renault, Jeffrey E. Dick

2024The Analyst10 citationsDOIOpen Access PDF

Abstract

= 6.3 μm). The aqueous phase serves as an infinite sink, enabling the dissolution of DCE droplets while also facilitating convenient electrical contact with the reference/counter electrode (Ag/AgCl 1 M KCl). Through comprehensive voltammetric analysis, we unravel the impact of droplet dissolution on electrochemical response as the droplet reaches minuscule volumes. We validate our experimental findings by finite element modelling, which shows deviations from the experimental results as the droplet accesses negligible volumes, suggesting the presence of complex dissolution modes.

Topics & Concepts

DissolutionVoltammetryCyclic voltammetryMaterials scienceChemistryChemical engineeringEngineeringElectrochemistryElectrodePhysical chemistryNanomaterials and Printing TechnologiesAdvanced Sensor and Energy Harvesting MaterialsInnovative Microfluidic and Catalytic Techniques Innovation
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