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Green Method for the Synthetic Ugi Reaction by Twin Screw Extrusion without a Solvent and Catalyst

Mahmoud Abd El Aleem Ali Ali El‐Remaily, Ahmed M. Soliman, Omar M. Elhady

2020ACS Omega41 citationsDOIOpen Access PDF

Abstract

This study describes the solvent and catalyst-free Ugi reaction by way of twin screw extrusion (TSE). Multicomponent chemical synthesis can be converted into a single process without repeated use of solvents through TSE. High synthetic yields are achieved in short reaction times and produced in solvent-free conditions, which lead to a more environmentally friendly process.

Topics & Concepts

ExtrusionCatalysisSolventEnvironmentally friendlyProcess (computing)Reaction conditionsReactive extrusionMaterials scienceChemical engineeringChemistryOrganic chemistryProcess engineeringComputer scienceMetallurgyEngineeringBiologyOperating systemEcologyMulticomponent Synthesis of HeterocyclesChemical Synthesis and AnalysisSynthesis and biological activity
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