Litcius/Paper detail

Distinct Reactivity Modes of a Copper Hydride Enabled by an Intramolecular Lewis Acid

Emily E. Norwine, John J. Kiernicki, Mat­thias Zeller, Nathaniel K. Szymczak

2022Journal of the American Chemical Society24 citationsDOIOpen Access PDF

Abstract

We disclose a 1,4,7-triazacyclononane (TACN) ligand featuring an appended boron Lewis acid. Metalation with Cu(I) affords a series of tetrahedral complexes including a boron-capped cuprous hydride. We demonstrate distinct reactivity modes as a function of chemical oxidation: hydride transfer to CO2 in the copper(I) state and oxidant-induced H2 evolution as well as alkyne reduction.

Topics & Concepts

ChemistryReactivity (psychology)HydrideMetalationIntramolecular forceAlkyneLewis acids and basesBoronCopperLigand (biochemistry)Inorganic chemistryPhotochemistryMedicinal chemistryStereochemistryOrganic chemistryHydrogenCatalysisPathologyMedicineAlternative medicineBiochemistryReceptorCarbon dioxide utilization in catalysisAsymmetric Hydrogenation and CatalysisOrganoboron and organosilicon chemistry