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Evaluation of 14-(p-tolyl)-14H-dibenzo[a,j]xanthene as a highly efficient organic corrosion inhibitor for mild steel in 1 M HCl: Electrochemical, theoretical, and surface characterization

Azzeddine Belkheiri, Khadija Dahmani, Mohamed Khattabi, Khaoula Mzioud, Otmane Kharbouch, M. Galai, Nadia Dkhireche, Zakaria Benzekri, Saı̈d Boukhris, Rafa Almeer, Basheer M. Al‐Maswari, M. Ebn Touhamı

2024International Journal of Electrochemical Science15 citationsDOIOpen Access PDF

Abstract

Corrosion of mild steel, particularly in acidic environments such as hydrochloric acid (HCl), remains a critical issue due to its impact on material durability, economic costs, and safety concerns. This study introduces 14-(p-tolyl)-14H-dibenzo[ a , j ]xanthene (ZM5), a novel and highly effective organic corrosion inhibitor, to mitigate this challenge. Employing advanced electrochemical techniques: electrochemical impedance spectroscopy (EIS) and potentiodynamic polarization (PDP), we evaluated ZM5’s performance in a 1 M HCl solution, revealing an impressive inhibition efficiency of 94.7 %. Surface characterization using scanning electron microscopy (SEM) and energy-dispersive X-ray spectroscopy (EDX) further confirmed the formation of a robust protective film on the steel surface, shedding light on ZM5’s adsorption mechanisms. Complementing the experimental findings, Density Functional Theory (DFT) simulations provided theoretical insights into the anti-corrosion mechanism of ZM5, aligning well with observed results. These findings underscore ZM5's potential as a highly promising corrosion inhibitor for industrial applications, effectively enhancing the corrosion resistance of mild steel in aggressive environments.

Topics & Concepts

XantheneElectrochemistryCharacterization (materials science)Materials scienceCorrosionCorrosion inhibitorChemical engineeringMetallurgyChemistryPhysical chemistryNanotechnologyOrganic chemistryElectrodeEngineeringCorrosion Behavior and InhibitionConcrete Corrosion and DurabilityHydrogen embrittlement and corrosion behaviors in metals
Evaluation of 14-(p-tolyl)-14H-dibenzo[a,j]xanthene as a highly efficient organic corrosion inhibitor for mild steel in 1 M HCl: Electrochemical, theoretical, and surface characterization | Litcius