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Photoredox radical/polar crossover enables C–H <i>gem</i>-difunctionalization of 1,3-benzodioxoles for the synthesis of monofluorocyclohexenes

Jiabao Tian, Lei Zhou

2023Chemical Science59 citationsDOIOpen Access PDF

Abstract

A sequential C–H gem -difunctionalization of 1,3-benzodioxoles with α-trifluoromethyl alkenes and electron-deficient alkenes in a redox-neutral radical polar crossover manifold have been developed for the synthesis of monofluorocyclohexenes.

Topics & Concepts

PolarChemistryCrossoverRadicalCombinatorial chemistryStereochemistryMedicinal chemistryOrganic chemistryComputer sciencePhysicsAstronomyArtificial intelligenceFluorine in Organic ChemistryRadical Photochemical ReactionsSulfur-Based Synthesis Techniques
Photoredox radical/polar crossover enables C–H <i>gem</i>-difunctionalization of 1,3-benzodioxoles for the synthesis of monofluorocyclohexenes | Litcius