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Multifunctional performance of Ti <sub>2</sub> AlC MAX phase/2D braided alumina fiber laminates

Jesús González‐Julián, Irina Kraleva, Manuel Belmonte, Fabian Jung, Thomas Gries, Raúl Bermejo

2021Journal of the American Ceramic Society11 citationsDOIOpen Access PDF

Abstract

Abstract The processing and characterization of laminates based on Ti 2 AlC MAX phase, as matrix, and triaxial alumina braids, as reinforcing phase, are presented. Ti 2 AlC powders with a mean particle size below 1 µm are synthesized, while commercial 3M Nextel 610 alumina fibers are braided in a three‐stage process consisting of spooling, braiding with an angle of 0° and ±60° and the separation to single‐layer fabric. The laminates are processed by layer‐by‐layer stacking, where 3 two‐dimensional alumina braids are interleaved between Ti 2 AlC layers, followed by full densification using a Field‐Assisted Sintering Technology/Spark Plasma Sintering. The multifunctional response of the laminates, as well as for the monolithic Ti 2 AlC, is evaluated, in particular, the thermal and electrical conductivity, the oxidation resistance, and the mechanical response. The laminates exhibit an anisotropic thermal and electrical behavior, and an excellent oxidation resistance at 1200℃ in air for a week. A relatively lower characteristic biaxial strength and Weibull modulus (i.e., σ 0 = 590 MPa and m = 9) for the laminate compared to the high values measured in the monolithic Ti 2 AlC (i.e., σ 0 = 790 MPa and m = 29) indicates the need but also the potential of optimizing MAX‐phase layered structures for multifunctional performance.

Topics & Concepts

Materials scienceComposite materialSpark plasma sinteringSinteringPhase (matter)StackingLayer (electronics)Thermal conductivityThermal shockOrganic chemistryChemistryPhysicsNuclear magnetic resonanceMXene and MAX Phase MaterialsAdvanced ceramic materials synthesisAluminum Alloys Composites Properties
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