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Electrochemical C-H Halogenations of Enaminones and Electron-Rich Arenes with Sodium Halide (NaX) as Halogen Source for the Synthesis of 3-Halochromones and Haloarenes

Yan Lin, Jun Jin, Chaoli Wang, Jie‐Ping Wan, Yunyun Liu

2021The Journal of Organic Chemistry69 citationsDOI

Abstract

Without employing an external oxidant, the simple synthesis of 3-halochromones and various halogenated electron-rich arenes has been realized with electrode oxidation by employing the simplest sodium halide (NaX, X = Cl, Br, I) as halogen source. This electrochemical method is advantageous for the simple and mild room temperature operation, environmental friendliness as well as broad substrate scope in both C-H bond donor and halogen source components.

Topics & Concepts

HalideHalogenElectrochemistryChemistrySubstrate (aquarium)Inorganic chemistrySodiumHalogenationElectrodeCombinatorial chemistryOrganic chemistryPhysical chemistryGeologyAlkylOceanographyRadical Photochemical ReactionsCatalytic C–H Functionalization MethodsOxidative Organic Chemistry Reactions
Electrochemical C-H Halogenations of Enaminones and Electron-Rich Arenes with Sodium Halide (NaX) as Halogen Source for the Synthesis of 3-Halochromones and Haloarenes | Litcius