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Copper-Mediated Decarboxylative Coupling between Arylacetic Acids and 1,3-Dicarbonyl Compounds

Yinrong Wu, Kangmei Wen, Jiewen Chen, Jie Shi, Xingang Yao, Xiaodong Tang

2021Organic Letters16 citationsDOI

Abstract

A copper-mediated decarboxylative coupling reaction between arylacetic acids and 1,3-dicarbonyl compounds was described. Significantly, methanocycloocta[b]indoles were also obtained by sequential intramolecular dehydrocyclization process in some cases. This protocol featured a broad substrate scope, simple operations, and good yields. Moreover, the products exhibited potent antiproliferative activity against the human cancer cell lines by a MTT assay.

Topics & Concepts

ChemistryIntramolecular forceSubstrate (aquarium)DecarboxylationCombinatorial chemistryCopperCoupling (piping)MTT assayOrganic chemistryCatalysisCell growthBiochemistryOceanographyGeologyEngineeringMechanical engineeringCatalytic C–H Functionalization MethodsCyclopropane Reaction MechanismsCatalytic Cross-Coupling Reactions