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Thermodynamic and Kinetic Influence of Oxygen Vacancies on the Solar Water Oxidation Reaction of α-Fe<sub>2</sub>O<sub>3</sub> Photoanodes

Qian Yang, Jinyan Du, Jie Li, Yuting Wu, Yong Zhou, Yang Yang, Dingming Yang, Huichao He

2020ACS Applied Materials & Interfaces68 citationsDOI

Abstract

To reveal the role of oxygen vacancies in the solar water oxidation of α-Fe2O3 photoanodes, the kinetic and thermodynamic properties that are closely related to the water oxidation reaction of the α-Fe2O3 photoanode containing oxygen vacancies were investigated. Compared with the pristine α-Fe2O3 photoanode, the presence of surface oxygen vacancies can improve the water oxidation activity and stability of the α-Fe2O3 photoanode simultaneously, but the bulk oxygen vacancies have a negative effect on the water oxidation performance of the α-Fe2O3 photoanode. In thermodynamics, our investigations revealed that the presence of surface oxygen vacancies narrows the space charge region width of the α-Fe2O3 photoanode, which could boost the charge separation and transfer efficiency of the α-Fe2O3 photoanode during water oxidation. Because the surface property and hydrophilicity of α-Fe2O3 are modified owing to the presence of surface oxygen vacancies, the water oxidation kinetics of the α-Fe2O3 photoanode with surface oxygen vacancies is obviously boosted. Our findings in the present work provide comprehensive understanding of the thermodynamic and kinetic differences for α-Fe2O3 photoanodes with and without oxygen vacancies for solar water oxidation.

Topics & Concepts

OxygenMaterials scienceOxygen evolutionRedoxChemical engineeringWater splittingKinetic energyKineticsInorganic chemistryChemical physicsCatalysisPhysical chemistryChemistryElectrochemistryPhotocatalysisElectrodeOrganic chemistryQuantum mechanicsEngineeringBiochemistryMetallurgyPhysicsIron oxide chemistry and applicationsMinerals Flotation and Separation TechniquesCopper-based nanomaterials and applications