Synthesis of sulfide solid electrolytes from Li<sub>2</sub>S and P<sub>2</sub>S<sub>5</sub> in anisole
Riku Maniwa, Marcela Calpa, Nataly Carolina Rosero‐Navarro, Akira Miura, Kiyoharu Tadanaga
Abstract
We report the liquid-phase synthesis of sulfide solid electrolytes from Li<sub>2</sub>S and P<sub>2</sub>S<sub>5</sub> using anisole at 200–300 °C under microwave irradiation, in which β-Li<sub>3</sub>PS<sub>4</sub> and Li<sub>7</sub>P<sub>3</sub>S<sub>11</sub> were directly precipitated in anisole in 30 min.
Topics & Concepts
AnisoleSulfideInorganic chemistryFast ion conductorChemistryMaterials scienceElectrolytePhysical chemistryCatalysisOrganic chemistryElectrodeAdvanced Battery Materials and TechnologiesAdvancements in Battery MaterialsThermal Expansion and Ionic Conductivity