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Cysteic acid grafted to magnetic graphene oxide as a promising recoverable solid acid catalyst for the synthesis of diverse 4H-chromene

Firouz Matloubi Moghaddam, Mohammad Eslami, Golfamsadat Hoda

2020Scientific Reports28 citationsDOIOpen Access PDF

Abstract

4H-chromenes play a significant role in natural and pharmacological products. Despite continuous advances in the synthesis methodology of these compounds, there is still a lack of a green and efficient method. In this study, we have designed cysteic acid chemically attached to magnetic graphene oxide (MNPs·GO-CysA) as an efficient and reusable solid acid catalyst to synthesize 4H-chromene skeletons via a one-pot three components reaction of an enolizable compound, malononitrile, an aldehyde or isatin, and a mixture of water-ethanol as a green solvent. This new heterogeneous catalyst provides desired products with a good to excellent yield, short time, and mild condition. This procedure presents an environmentally friendly approach for the synthesis of a great number of 4H-chromene derivatives.

Topics & Concepts

MalononitrileIsatinCysteic acidCatalysisYield (engineering)OxideAldehydeGrapheneChemistryEnvironmentally friendlyEthanolCombinatorial chemistryOrganic chemistryNanotechnologyMaterials scienceEcologyCystineMetallurgyCysteineBiologyEnzymeMulticomponent Synthesis of HeterocyclesSynthesis of Organic CompoundsSynthesis and biological activity
Cysteic acid grafted to magnetic graphene oxide as a promising recoverable solid acid catalyst for the synthesis of diverse 4H-chromene | Litcius