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Stable Zinc(II) Coordination Polymer as a Rapid and Highly Sensitive Fluorescence Sensor for the Discriminative Sensing of Biomarker 2-(2-Methoxyethoxy) Acetic Acid

Yue Wang, Na Xu, Jianxin Ma, Hui Li, Yue Zhang, Guo‐Cheng Liu, Xiuli Wang

2022Inorganic Chemistry20 citationsDOI

Abstract

A novel two-dimensional bilayer Zn-based luminescent coordination polymer (LCP) [Zn2(μ2-OH)(4-dptp)(3,4′,5-bpt)] (LCP 1) [4-dptp = N3,N4-bis(pyridin-4-ylmethyl)thiophene-3,4-dicarboxamide and 3,4′,5-H3bpt = biphenyl-3,4′,5-tricarboxylic acid] was successfully prepared under hydrothermal conditions and characterized by single-crystal X-ray diffraction, IR spectroscopy, powder X-ray diffraction, and luminescence spectroscopy. LCP 1 displayed excellent fluorescence-quenching efficiency toward a biomarker 2-(2-methoxyethoxy) acetic acid (MEAA) with a high Ksv (5.153 × 104 M–1), a low limit of detection (0.244 μM), and a rapid response time (28 s). Additionally, LCP 1 can repeatedly detect MEAA at least eight times with excellent stability. The sensing mechanism was also carefully investigated through UV–vis absorption spectroscopy, density functional theory calculations, and fluorescence lifetime analysis.

Topics & Concepts

ChemistryFluorescenceFluorescence spectroscopyAcetic acidLuminescenceDetection limitQuenching (fluorescence)PolymerSpectroscopyAbsorption spectroscopyZincNuclear chemistryOrganic chemistryChromatographyMaterials scienceQuantum mechanicsOptoelectronicsPhysicsMetal-Organic Frameworks: Synthesis and ApplicationsMolecular Sensors and Ion DetectionLuminescence and Fluorescent Materials