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Electrochemical Nitration with Nitrite

Stephan P. Blum, Christean Nickel, Lukas Schäffer, Tarik Karakaya, Siegfried R. Waldvogel

2021ChemSusChem38 citationsDOIOpen Access PDF

Abstract

Abstract Aromatic nitration has tremendous importance in organic chemistry as nitroaromatic compounds serve as versatile building blocks. This study represents the electrochemical aromatic nitration with NBu 4 NO 2 , which serves a dual role as supporting electrolyte and as a safe, readily available, and easy‐to‐handle nitro source. Stoichiometric amounts of 1,1,1‐3,3,3‐hexafluoroisopropan‐2‐ol (HFIP) in MeCN significantly increase the yield by solvent control. The reaction mechanism is based on electrochemical oxidation of nitrite to NO 2 , which initiates the nitration reaction in a divided electrolysis cell with inexpensive graphite electrodes. Overall, the reaction is demonstrated for 20 examples with yields of up to 88 %. Scalability is demonstrated by a 13‐fold scale‐up.

Topics & Concepts

NitrationElectrochemistryElectrolysisChemistryNitriteYield (engineering)NitroElectrolyteOrganic chemistryCombinatorial chemistryInorganic chemistryElectrodeMaterials scienceNitratePhysical chemistryMetallurgyAlkylRadical Photochemical ReactionsSulfur-Based Synthesis TechniquesAmmonia Synthesis and Nitrogen Reduction
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