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Nitrene formation is the first step of the thermal and photochemical decomposition reactions of organic azides

Juan Soto, Manuel Algarra, Daniel Peláez

2022Physical Chemistry Chemical Physics30 citationsDOIOpen Access PDF

Abstract

, respectively. To complete this study, the kinetics of the singlet and triplet channels are modeled with the MESMER (Master Equation Solver for Multi-Energy Well Reactions) code by applying the RRKM and Landau-Zener (with WKB tunnelling correction) theories, respectively. It is found that the canonical rate-coefficients of the singlet path are 2-orders of magnitude higher than the rate-coefficients of the forbidden reaction. In addition, the concerted mechanism has been investigated that would lead to the formation of the imine derivative and nitrogen extrusion in the first step of the decomposition. After a careful analysis of CASSCF calculations with different active spaces and their comparison with single electronic configuration methods (MP2 and B3LYP), the concerted mechanism is discarded.

Topics & Concepts

NitrenePhotochemistryChemistryThermal decompositionDecompositionThermalOrganic chemistryCatalysisThermodynamicsPhysicsChemical Reactions and MechanismsAdvanced Chemical Physics StudiesSynthesis and Catalytic Reactions
Nitrene formation is the first step of the thermal and photochemical decomposition reactions of organic azides | Litcius