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Biosourced Aromatic Derivatives in the Upcycling of Recycled PET: Mellophanic Dianhydride as a Chain Extender

Ada M. Truscello, S. L. COLLETTI, Cristian Gambarotti, Marco Aldo Ortenzi, Stefano Gazzotti, Maurizio Galimberti

2023ACS Sustainable Chemistry & Engineering14 citationsDOIOpen Access PDF

Abstract

High Resolution Image Download MS PowerPoint Slide The synthesis of mellophanic dianhydride (MEDA) from biosourced 1,2,3,4-benzene tetracarboxylic derivatives and its use as a chain extender for mechanically recycled PET (R-PET) as an alternative to traditional oil-based pyromellitic dianhydride (PMDA) is reported. The rheological tests performed on the R-PET extruded with MEDA have shown similar results to those obtained with PMDA, and dynamic mechanical thermal analysis (DMTA) showed that, in the 90–110 °C range (i.e., the temperature range commonly used for blow molding of bottles), Young’s modulus of R-PET containing MEDA is about 20% higher in comparison to that of pristine R-PET. The advantage of MEDA is that it can be prepared using building blocks obtained from agricultural waste via a sustainable protocol, whereas PMDA is a product of oil-based chemistry.

Topics & Concepts

Pyromellitic dianhydrideExtenderDynamic mechanical analysisMaterials scienceRaw materialOrganic chemistryPolyimideChemistryChemical engineeringPolymer chemistryPolyurethanePolymerLayer (electronics)Engineeringbiodegradable polymer synthesis and propertiesPolymer crystallization and propertiesCatalysis for Biomass Conversion
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