Litcius/Paper detail

Development of a universal nanobody-binding Fab module for fiducial-assisted cryo-EM studies of membrane proteins

Joël S. Bloch, Somnath Mukherjee, Julia Kowal, E.V. Filippova, Martina Niederer, Els Pardon, Jan Steyaert, Anthony A. Kossiakoff, Kaspar P. Locher

2021Proceedings of the National Academy of Sciences117 citationsDOIOpen Access PDF

Abstract

Significance Structural studies of membrane proteins by cryogenic electron microscopy (cryo-EM) often require antibody fragments (Fabs) to facilitate particle alignments and achieve high resolution. While conformational nanobodies have been developed to lock specific states of many membrane proteins, they only add 15 kDa of mass to the complex. We developed a synthetic Fab (NabFab) that rigidly binds the conserved scaffold of nanobodies, providing a universally applicable fiducial for cryo-EM studies of protein–nanobody complexes. We demonstrate the concept by determining two high-resolution structures of membrane proteins bound to specific nanobodies and NabFab. As the structural epitope for NabFab can be incorporated into the scaffold of virtually any nanobody, this raises the prospect of facile structure determination of many nanobody–protein complexes.

Topics & Concepts

Cryo-electron microscopyEpitopeFiducial markerMembrane proteinBiophysicsChemistryMembraneResolution (logic)Scaffold proteinComputational biologyNanotechnologyCrystallographyAntibodyBiologyBiochemistryMaterials scienceComputer scienceImmunologyArtificial intelligenceSignal transductionMonoclonal and Polyclonal Antibodies ResearchAdvanced Electron Microscopy Techniques and ApplicationsBiochemical and Structural Characterization