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<i>Aza</i>-Quasi-Favorskii Reaction: Construction of Highly Substituted Aziridines through a Concerted Multibond Rearrangement Process

Padmanabha V. Kattamuri, Jidong Zhao, Tamal Das, Juha H. Siitonen, Nathan Morgan, Daniel H. Ess, László Kürti

2022Journal of the American Chemical Society15 citationsDOIOpen Access PDF

Abstract

A new molecular rearrangement, the aza-Quasi-Favorskii rearrangement, has been developed for the construction of highly substituted aziridines. Electron-deficient O-sulfonyl oximes react readily with α,α-disubstituted acetophenone-derived enolates to furnish highly substituted aziridines via this unprecedented domino process. In-depth computational studies reveal an asynchronous yet concerted nitrenoid-type rearrangement pathway.

Topics & Concepts

ChemistryAcetophenoneSigmatropic reactionCope rearrangementSulfonylPericyclic reactionConcerted reactionAziridineComputational chemistryCombinatorial chemistryMedicinal chemistryOrganic chemistryRing (chemistry)CatalysisAlkylSynthesis and Catalytic ReactionsCatalytic C–H Functionalization MethodsSulfur-Based Synthesis Techniques