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Base-Promoted Multicomponent Reactions: A Synthesis of 2-Amino-1,3-selenazole Derivatives

Huawei Liu, Yi Fang, Shun‐Yi Wang, Shun‐Jun Ji

2020The Journal of Organic Chemistry28 citationsDOI

Abstract

New practical synthesis of 2-amino-1,3-selenazole with transition metal-free multicomponent reaction is reported here. A series of 2-amino-1,3-selenazole derivatives were afforded by the nucleophilic addition of amines to isoselenocyanate formed in situ, followed by Michael addition reaction and aromatization. The products were isolated from moderate to excellent yields.

Topics & Concepts

ChemistryAromatizationNucleophilic additionNucleophileBase (topology)Michael reactionTransition metalNucleophilic substitutionCombinatorial chemistryOrganic chemistryCatalysisMathematicsMathematical analysisOrganoselenium and organotellurium chemistrySulfur-Based Synthesis TechniquesSynthesis and biological activity