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Chemical Affinity of Ag-Exchanged Zeolites for Efficient Hydrogen Isotope Separation

Linda Zhang, Toshiki Wulf, Florian Baum, Wolfgang Schmidt, Thomas Heine, Michael Hirscher

2022Inorganic Chemistry34 citationsDOIOpen Access PDF

Abstract

selectivity of 10 is found at an exposure temperature of 90 K. Furthermore, the high Al content of the zeolite structure leads to a high density of Ag sites, resulting in a high gas uptake. In the framework, approximately one-third of the total physisorbed hydrogen isotopes are adsorbed on the Ag sites, corresponding to 3 mmol/g. A density functional theory (DFT) calculation reveals that the isotopologue-selective adsorption of hydrogen at Ag sites contributes to the outstanding hydrogen isotope separation, which has been directly observed through cryogenic thermal desorption spectroscopy. The overall performance of zeolite AgY, showing good selectivity combined with high gas uptake, is very promising for future technical applications.

Topics & Concepts

ChemistryZeoliteIsotopologueHydrogenAdsorptionDesorptionSelectivityIon exchangeThermal desorptionAnalytical Chemistry (journal)Inorganic chemistrySpectroscopyThermal desorption spectroscopyDensity functional theoryPhysical chemistryCatalysisIonMoleculeOrganic chemistryComputational chemistryQuantum mechanicsPhysicsChemical Synthesis and CharacterizationHydrogen Storage and MaterialsAmmonia Synthesis and Nitrogen Reduction