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A Lanthanum‐Filled Carbon–Boron Clathrate

Timothy A. Strobel, Li Zhu, Piotr A. Guńka, Gustav M. Borstad, Michael Guerette

2020Angewandte Chemie International Edition27 citationsDOIOpen Access PDF

Abstract

Abstract We report a carbon‐boron clathrate with composition 2 La@B 6 C 6 (LaB 3 C 3 ). Like recently reported SrB 3 C 3 , [1] single‐crystal X‐ray diffraction and computational modelling indicate that the isostructural La member crystallizes in the cubic bipartite sodalite structure (Type‐VII clathrate) with La atoms encapsulated within truncated octahedral cages composed of alternating carbon and boron atoms. The covalent nature of the B−C bonding results in a hard, incompressible framework, and owing to the balanced electron count, La 3+ [B 3 C 3 ] 3− exhibits markedly improved pressure stability and is a semiconductor with an indirect band gap predicted near 1.3 eV. A variety of different guest atoms may potentially be substituted within Type‐VII clathrate cages, presenting opportunities for a large family of boron‐stabilized, carbon‐based clathrates with ranging physical properties.

Topics & Concepts

Clathrate hydrateIsostructuralCrystallographyBoronOctahedronLanthanumCarbon fibersSodaliteMaterials scienceCrystal structureChemistryInorganic chemistryHydrateOrganic chemistryComposite materialZeoliteComposite numberCatalysisMXene and MAX Phase MaterialsBoron and Carbon Nanomaterials ResearchInorganic Chemistry and Materials