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Remote Arylative Substitution of Alkenes Possessing an Acetoxy Group via β‐Acetoxy Elimination

Kazuma Muto, T Kumagai, Fumitoshi Kakiuchi, Takuya Kochi

2021Angewandte Chemie International Edition19 citationsDOI

Abstract

Palladium-catalyzed remote arylative substitution was achieved for the reaction of arylboronic acids with alkenes possessing a distant acetoxy group to provide arylation products having an alkene moiety at the remote position. The use of β-acetoxy elimination as a key step in the catalytic cycle allowed for regioselective formation of unstabilized alkenes after chain walking. This reaction was applicable to various arylboronic acids as well as alkene substrates.

Topics & Concepts

AlkeneRegioselectivityMoietyChemistryPalladiumCatalysisSubstitution reactionFunctional groupOrganic chemistryCombinatorial chemistryPolymerCatalytic C–H Functionalization MethodsCatalytic Cross-Coupling ReactionsRadical Photochemical Reactions
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