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Electron Paramagnetic Resonance for the Detection of Electrochemically Generated Hydroxyl Radicals: Issues Associated with Electrochemical Oxidation of the Spin Trap

Emily Braxton, David J. Fox, Ben G. Breeze, Joshua J. Tully, Katherine J. Levey, Mark E. Newton, Julie V. Macpherson

2022ACS Measurement Science Au55 citationsDOIOpen Access PDF

Abstract

-butylnitrone, and 2-methyl-2-nitrosopropane dimer, also show electrochemical oxidation signals less positive than that of water on a BDD electrode. Such behavior also complicates their use for the intended application.

Topics & Concepts

ChemistryElectron paramagnetic resonanceRadicalElectrochemistryAdductSpin trappingAqueous solutionOxideInorganic chemistryOxidizing agentPhotochemistryElectrodeAnalytical Chemistry (journal)Nuclear magnetic resonancePhysical chemistryOrganic chemistryPhysicsElectron Spin Resonance StudiesAnalytical Chemistry and SensorsElectrochemical Analysis and Applications
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