Litcius/Paper detail

Grain size, crystalline phase and fracture toughness of the monolithic zirconia

Kodchakorn Bocam, Chuchai Anunmana, Trinuch Eiampongpaiboon

2022The Journal of Advanced Prosthodontics18 citationsDOIOpen Access PDF

Abstract

PURPOSE: This study evaluated the relationship among translucency, crystalline phase, grain size, and fracture toughness of zirconia. MATERIALS AND METHODS: (P), InCorisZI (ZI), and InCorisTZI (TZI)- were selected for this study. The bar specimens were prepared to determine fracture toughness by using chevron notched beam method with four-point bending test. The grain size was evaluated by a mean linear intercept method using a scanning electron microscope. X-ray diffraction and Rietveld refinement were performed to evaluate the amount of tetragonal and cubic phases of zirconia. Contrast ratio (CR) was measured to investigate the level of translucency. RESULTS: < .05). This means PA was the most translucent material in this study. Rietveld refinement found that PA presented the greatest percentage of cubic phase, followed by TZI, ZI, and P, respectively. CONCLUSION: The different approaches are used by manufacturers to fabricate various types of translucent zirconia with different levels of translucency and mechanical properties, which should be concerned for material selection for successful clinical outcome.

Topics & Concepts

Fracture toughnessMaterials scienceGrain sizeCubic zirconiaRietveld refinementScanning electron microscopeComposite materialTetragonal crystal systemAnalytical Chemistry (journal)CrystallographyCeramicCrystal structureChemistryChromatographyDental materials and restorationsAdvanced ceramic materials synthesisBone Tissue Engineering Materials