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Utilization of Machine Learning for the Differentiation of Positional NPS Isomers with Direct Analysis in Real Time Mass Spectrometry

Jennifer L. Bonetti, Saer Samanipour, Arian van Asten

2022Analytical Chemistry33 citationsDOIOpen Access PDF

Abstract

test at each included ion; a multivariate approach, linear discriminant analysis; and a machine learning approach, the Random Forest classifier. For each method, multiple validation techniques were used including restricting the classifier to data that was only generated on one day. Of these classification methods, the Random Forest algorithm was ultimately the most accurate and robust, consistently achieving out-of-bag error rates below 5%. At an inconclusive rate of approximately 5%, a success rate of 100% was obtained for isomer identification when applied to a randomly selected test set. The model was further tested with data acquired as a part of a different batch. The highest classification success rate was 93.9%, and error rates under 5% were consistently achieved.

Topics & Concepts

ChemistryRandom forestStructural isomerLinear discriminant analysisMass spectrometryUnivariateDART ion sourceArtificial intelligenceClassifier (UML)Pattern recognition (psychology)Multivariate statisticsChromatographyMachine learningComputer scienceStereochemistryIonIonizationElectron ionizationOrganic chemistryMass Spectrometry Techniques and ApplicationsMetabolomics and Mass Spectrometry StudiesAnalytical Chemistry and Chromatography
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