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Oxysulfonylation of Alkynes with Sodium Sulfinates to Access β-Keto Sulfones Catalyzed by BF3·OEt2

Shi‐Wei Yu, Zu-Jia Chen, Huanqing Li, Wenxi Li, Yun Li, Z. J. Li, Zhao‐Yang Wang

2024Molecules11 citationsDOIOpen Access PDF

Abstract

An efficient and operationally simple method for the synthesis of β-keto sulfones through the BF3·OEt2-promoted reaction of alkynes and sodium sulfinates is developed. With its facile and selective access to the targets, it features good functional group compatibility, mild conditions, easily available starting materials, and good yields. Notably, the reaction does not require metal catalysts or chemical reagents with pungent odors.

Topics & Concepts

CatalysisChemistrySodiumOrganic chemistrySulfur-Based Synthesis TechniquesChemical Synthesis and ReactionsCyberloafing and Workplace Behavior
Oxysulfonylation of Alkynes with Sodium Sulfinates to Access β-Keto Sulfones Catalyzed by BF3·OEt2 | Litcius