Litcius/Paper detail

Investigating the influence of strain rate on hydrogen embrittlement in steel sub-size tensile specimens using 3D X-ray tomography

Luciano Meirelles Santana, Victor Okumko, Andrew King, Thilo F. Morgeneyer, Jacques Besson, Yazid Madi

2025International Journal of Hydrogen Energy8 citationsDOIOpen Access PDF

Abstract

This study investigates the effect of strain rate on hydrogen embrittlement in ferritic-pearlitic E355 steel sub-size tensile specimens . Micrometer-scale damage analysis was performed using 3D X-ray tomography . Tests were conducted using an optical extensometry at varying strain rates in air and a 100 bar gas hydrogen atmosphere, including interrupted tests before rupture to capture damage states. Hydrogen reduces ductility, with losses reaching up to 62.8% at slower strain rates. At moderate strain rate , 5 × 10 −4 s −1 , surface damage manifests as brittle, flat ellipsoidal cracks perpendicular to the tensile axis , while the bulk retains ductile damage with prolate voids aligned longitudinally. Hydrogen-enhanced internal shearing leads to damage coalescence via slant fracture of the ligament between surface cracks and internal voids. At low strain rates (1 × 10 −5 s −1 ), deeper hydrogen diffusion induces brittle flat ellipsoidal cracks both at the surface and in the bulk.

Topics & Concepts

Hydrogen embrittlementMaterials scienceStrain rateUltimate tensile strengthEmbrittlementHydrogenStrain (injury)MetallurgyX-rayChemistryMedicinePhysicsCorrosionOrganic chemistryQuantum mechanicsInternal medicineHydrogen embrittlement and corrosion behaviors in metalsMicrostructure and Mechanical Properties of SteelsNuclear Materials and Properties