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Photocatalytic difluoromethylarylation of unactivated alkenes <i>via</i> a (hetero)aryl neophyl-like radical migration

Ziran Lei, Siqi Wei, Liejin Zhou, Zuxiao Zhang, Simón E. López, William R. Dolbier

2022Organic & Biomolecular Chemistry16 citationsDOI

Abstract

Photoredox-catalyzed addition of the difluoromethylradical to unactivated alkenes has been found to trigger neophyl-like aryl and heteroaryl migrations which allowed the construction of a diverse series of difluoromethyl ketones. The reaction featured mild reaction conditions and broad substrate scope.

Topics & Concepts

ChemistryPhotocatalysisArylPhotochemistryAryl radicalCombinatorial chemistryOrganic chemistryCatalysisAlkylFluorine in Organic ChemistryRadical Photochemical ReactionsSulfur-Based Synthesis Techniques
Photocatalytic difluoromethylarylation of unactivated alkenes <i>via</i> a (hetero)aryl neophyl-like radical migration | Litcius