Litcius/Paper detail

Addition of Fluorine and a Late-Stage Functionalization (LSF) of the Oral SERD AZD9833

James S. Scott, Tom Moss, Bernard Barlaam, Paul R. J. Davey, Gary Fairley, Eric T. Gangl, Ryan Greenwood, Holia Hatoum‐Mokdad, Andrew Lister, David Longmire, Radosław Polański, S.P. Stokes, Michael Tucker, Jeffrey Varnes, Bin Yang

2020ACS Medicinal Chemistry Letters20 citationsDOIOpen Access PDF

Abstract

Herein we describe our efforts using a late stage functionalization together with more traditional synthetic approaches to generate fluorinated analogues of the clinical candidate AZD9833. The effects of the addition of fluorine on the lipophilicity, permeability, and metabolism are discussed. Many of these changes were tolerated in terms of pharmacology and resulted in high quality molecules which reached advanced stages of profiling in the testing cascade.

Topics & Concepts

LipophilicitySurface modificationCascadeFluorineCombinatorial chemistryChemistryComputer scienceStereochemistryOrganic chemistryPhysical chemistryChromatographyFluorine in Organic ChemistryChemical Synthesis and AnalysisClick Chemistry and Applications