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Tuning of Redox Potentials and LUMO Levels of BODIPYs via Site-Selective Direct Cyanation

Huiquan Zuo, Qinghua Wu, Xing Guo, Zhengxin Kang, Jiangang Gao, Ying Wei, Changjiang Yu, Lijuan Jiao, Erhong Hao

2023Organic Letters15 citationsDOI

Abstract

promoted oxidative nucleophilic hydrogen substitution, site-selective direct and stepwise cyanation of BODIPYs using tetrabutylammonium cyanide was developed to give α-cyanated BODIPY derivatives. Characterization of optical and electrochemical properties of these dyes provides substantial enhancement of the electron affinity, with a reduction potential and LUMO level as low as -0.04 V and -4.43 eV, respectively. Radical anions of these electron-deficient 3,5-dicyanated BODIPYs were characterized by absorption and EPR spectroscopy.

Topics & Concepts

ChemistryCyanationHOMO/LUMOPhotochemistryRedoxCyanideElectrochemistryInorganic chemistryOrganic chemistryMoleculeCatalysisElectrodePhysical chemistryLuminescence and Fluorescent MaterialsOrganic Light-Emitting Diodes ResearchConducting polymers and applications
Tuning of Redox Potentials and LUMO Levels of BODIPYs via Site-Selective Direct Cyanation | Litcius