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Dual Modification Strategy: Passivation Layer and Cocatalyst on Hematite for Improved Photoelectrochemical Water Oxidation

Zhi Yin, Xueyang Leng, Dutong Wang, Lingling Xu

2024ACS Applied Materials & Interfaces11 citationsDOI

Abstract

α-Fe 2 O 3 is a very attractive photoanode for photoelectrochemical (PEC) water decomposition. However, its short diffusion length, poor conductivity, and fast charge-carrier recombination severely limit device efficiency. Here, coloading an Al 2 O 3 passivation layer and a CoO x cocatalyst onto Ti-doped α-Fe 2 O 3 was carried out to promote PEC water oxidation by improving charge separation and transfer at the electrode/electrolyte interface and inhibiting photocarrier recombination. The optimized Ti:Fe 2 O 3 /Al 2 O 3 /CoO x photoanode shows a large photocurrent density of 1.41 mA cm –2 at 1.23 V vs reversible hydrogen electrode, which is 47 times greater than that of a pristine Ti:Fe 2 O 3 photoanode. The dual modifications with a combined passivation layer and cocatalyst on the photoanode verify a valuable way for solar energy conversion in PEC water oxidation.

Topics & Concepts

PassivationMaterials scienceHematiteLayer (electronics)Surface modificationWater splittingPhotoelectrochemistryDual layerDual (grammatical number)Anodic oxidationChemical engineeringInorganic chemistryNanotechnologyPhotocatalysisElectrochemistryCatalysisElectrodeMetallurgyOrganic chemistryChemistryPhysical chemistryLiteratureEngineeringArtIron oxide chemistry and applicationsAdvanced Photocatalysis TechniquesMine drainage and remediation techniques