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Electronically Activated Fe<sub>5</sub>C<sub>2</sub> via N-Doped Carbon to Enhance Photothermal Syngas Conversion to Light Olefins

Ruizhe Li, Yuan Li, Zhenhua Li, Weiqin Wei, Quanguo Hao, Yiqiu Shi, Shuxin Ouyang, Hong Yuan, Tierui Zhang

2022ACS Catalysis55 citationsDOI

Abstract

Solar-driven CO hydrogenation to light olefins holds great potential as a petroleum-independent process. Herein, a series of Fe5C2 loading on tunable N-doped carbon as photothermal catalysts are developed to achieve an efficient Fischer–Tropsch synthesis to olefin (FTO) reaction. Under light irradiation, the optimized catalyst delivers a selectivity of 55.3% for light olefins (CO2 free) at a CO conversion of 22.3%, showing 3.5 times the activity of pristine Fe5C2 catalyst. Experimental characterizations reveal electron transfer from the N atoms in support to the active phase of Fe5C2 to construct electron-rich active sites and therefore to boost the catalytic performance. N-concentration-dependent activity evaluation and density functional theory calculations ascertain that pyrrolic N plays a dominant role in promoting CO adsorption and activation. This study provides an alternative strategy of rational modulation of support to enhance solar-to-chemical conversion.

Topics & Concepts

CatalysisOlefin fiberSyngasActivated carbonSelectivityAdsorptionMaterials scienceCarbon fibersChemical engineeringPhotochemistryPhotothermal therapyElectron transferDopingDensity functional theoryChemistryNanotechnologyPhysical chemistryOrganic chemistryComputational chemistryOptoelectronicsComposite numberEngineeringComposite materialCatalysts for Methane ReformingCatalytic Processes in Materials ScienceElectrocatalysts for Energy Conversion